Ammonium fluoroperoxomonophosphate dihydrate, [NH4]2[PO2(O2)F]·2H2O. First chemical synthesis of a fluorinated peroxophosphate (Englisch)

Journal of the Chemical Society, Dalton Transactions
; 1988
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The salt [NH4]2[PO2(O2)F]·2H2O has been synthesised from the reaction of [NH4][H2PO4] with 48% HF and 30% H2O2 at pH 10–11, maintained by the addition of aqueous ammonia, at an ice-bath temperature. The compound has been characterised by chemical analysis, i.r., and laser-Raman spectroscopic studies. Some properties of the compound are also reported.

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