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Inhaltsverzeichnis
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Cobalt salt-catalyzed carbocyclization reactions of α-bromo-N-phenylacetamide derivativesElectronic supplementary information (ESI) available: Experimental details and characterization data for starting α-bromo-N-phenylacetamides 1 and 4; 1H and 13C NMR spectra of 2-quinolinones 2 and 5 and radical-trapping adducts 7a and 8a. See DOI: 10.1039/c7ob00009j
Diastereoselective synthesis of tetrahydropyrans via Prins-Ritter and Prins-arylthiolation cyclization reactionsElectronic supplementary information (ESI) available: 1H and 13C NMR spectra of all compounds, and NOESY spectrum of 7da. CCDC 1502070. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c6ob02692c
Photocatalytic esterification under Mitsunobu reaction conditions mediated by flavin and visible lightElectronic supplementary information (ESI) available: Experimental section and copies of NMR spectra and HPLC chromatograms. See DOI: 10.1039/c6ob02770a
Whole cell-SELEX of aptamers with a tyrosine-like side chain against live bacteriaElectronic supplementary information (ESI) available: Tables and figures presenting the selection conditions, the enrichment numbers, the sequencing data and the raw data for the selectivity and saturation binding assays. See DOI: 10.1039/c6ob02451c
Formation of β-(1,3-1,6)-d-glucan-complexed [70]fullerene and its photodynamic activity towards macrophagesElectronic supplementary information (ESI) available: TEM images. See DOI: 10.1039/c6ob02747d
Enantioselective synthesis of spiro γ-butyrolactones by N-heterocyclic carbene (NHC)-catalyzed formal [3 + 2] annulation of enals with 3-hydroxy oxindolesElectronic supplementary information (ESI) available: Details on the experimental procedure, characterization data and HPLC data of all compounds, detailed mechanistic investigation, and single crystal X-ray data of compound 3n. CCDC 1487677. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c7ob00148g
Discovery of (S)-3′-hydroxyblebbistatin and (S)-3′-aminoblebbistatin: polar myosin II inhibitors with superior research tool propertiesElectronic supplementary information (ESI) available: Synthetic protocols and compound characterization of compounds 4b, 4c, S5, 6a-d, 10, 7, 8a-d and 9a-d; X-ray crystallographic data of (S)-2 and (R)-2; 1H NMR spectra and 13C NMR spectra; chiral HPLC chromatograms; additional data relating to ATPase assay and microscopic imaging of fluorescence. Crystallographic data (CCDC 1485738 and 1485739) in CIF or other electronic format see DOI: 10.1039/c7ob00006e
Amphipathic guanidine-embedded glyoxamide-based peptidomimetics as novel antibacterial agents and biofilm disruptorsElectronic supplementary information (ESI) available. See DOI: 10.1039/c7ob00053g
One-pot construction of sterically challenging and diverse polyarylphenols via transition-metal-free benzannulation and their potent in vitro antioxidant activityElectronic supplementary information (ESI) available: 1H NMR and 13C NMR spectra for synthesized compounds. X-ray structure and data for 9d. CCDC 1526470. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c7ob00078b
Catalyst free synthesis of α-fluoro-β-hydroxy ketones/α-fluoro-ynols via electrophilic fluorination of tertiary propargyl alcohols using Selectfluor™ (F-TEDA-BF4)Electronic supplementary information (ESI) available: Copies of the NMR spectra of the new compounds. CCDC 1033721. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c7ob00140a
3′-Pyrene-modified unlocked nucleic acids: synthesis, fluorescence properties and a surprising stabilization effect on duplexes and triplexesElectronic supplementary information (ESI) available: NMR spectra of new compounds, CD spectra, fluorescence spectra and UV/VIS absorbance spectra. See DOI: 10.1039/c6ob02773c
Synthesis, radio-synthesis and in vitro evaluation of terminally fluorinated derivatives of HU-210 and HU-211 as novel candidate PET tracersElectronic supplementary information (ESI) available. See DOI: 10.1039/c6ob02796b
Synthesis of 8-azaprotosappanin A derivatives via intramolecular palladium-catalyzed ortho C–H activation/C–C cyclization and their antibacterial activity
Diastereoselective tandem oxidation/Michael/aldol reaction: unprecedented formation of dispirocyclopentanebisoxindoles and dispiro[acenaphthylene-1,1′-cyclopentane-3′,1′′-acenaphthylene]-2,2′′diones
Diastereoselective tandem oxidation/Michael/aldol reaction: unprecedented formation of dispirocyclopentanebisoxindoles and dispiro[acenaphthylene-1,1′-cyclopentane-3′,1′′-acenaphthylene]-2,2′′dionesElectronic supplementary information (ESI) available: 1H, 13C and Dept-135 NMR spectra of compounds 2a-l and 4a-d. Crystallographic data of compound 2a. CCDC 1413924 (2a). For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c6ob02607a
Diastereoselective tandem oxidation/Michael/aldol reaction: unprecedented formation of dispirocyclopentanebisoxindoles and dispiro[acenaphthylene-1,1prime-cyclopentane-3prime,1primeprime-acenaphthylene]-2,2primeprimediones
Suman, K.
/ Ramanjaneyulu, M.
/ Thennarasu, S.et al.
| 2017
Synthesis of alkynyl furoxans. Rare carbon-carbon bond-forming reaction on a furoxan ringElectronic supplementary information (ESI) available: Typical experimental procedures, characterization of new compounds, copies of 1H and 13C NMR. CCDC 1520634 and 1521390. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c7ob00181a
Viability of dodecahedrane-forming radical polycyclizationsElectronic supplementary information (ESI) available: Coordinates and energies for computed structures, data for reactions not described in detail in the text. See DOI: 10.1039/c6ob02300b
Enantioselective synthesis of spiro g-butyrolactones by N-heterocyclic carbene (NHC)-catalyzed formal [3 + 2] annulation of enals with 3-hydroxy oxindoles
Mukherjee, S.
/ Joseph, S.
/ Bhunia, A.et al.
| 2017
Enantioselective synthesis of spiro γ-butyrolactones by N-heterocyclic carbene (NHC)-catalyzed formal [3 + 2] annulation of enals with 3-hydroxy oxindoles
One-pot construction of sterically challenging and diverse polyarylphenols via transition-metal-free benzannulation and their potent in vitro antioxidant activity
Maezono, Shizuka Mei Bautista
/ Poudel, Tej Narayan
/ Lee, Yong Roket al.
| 2017
Catalyst free synthesis of α-fluoro-β-hydroxy ketones/α-fluoro-ynols via electrophilic fluorination of tertiary propargyl alcohols using Selectfluor™ (F-TEDA-BF4)
Catalyst free synthesis of a-fluoro-b-hydroxy ketones/a-fluoro-ynols via electrophilic fluorination of tertiary propargyl alcohols using Selectfluor (F-TEDA-BF4)
Post-synthetic conversion of 5-pivaloyloxymethyluridine present in a support-bound RNA oligomer into biologically relevant derivatives of 5-methyluridine
Correction: Intermolecular interactions boost aggregation induced emission in carbazole Schiff base derivativesElectronic supplementary information (ESI) available. CCDC 1487394 (1), 1487391 (2), 1487392 (3), 1487393 (5) and 1447868 (6), respectively. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c6ob02181f
Post-synthetic conversion of 5-pivaloyloxymethyluridine present in a support-bound RNA oligomer into biologically relevant derivatives of 5-methyluridineElectronic supplementary information (ESI) available: Synthesis and spectral analysis of 5 and 6; procedures of 5′-depivaloylation of 11; HPLC analysis and spectral identification of Pivom5U-RNAs and xm5U-RNAs. See DOI: 10.1039/c6ob02674e
Three-component difunctionalization of alkenes leading to β-acetamido sulfides and β-acetoxy sulfidesElectronic supplementary information (ESI) available. See DOI: 10.1039/c7ob00110j
Synthesis of 8-azaprotosappanin A derivatives via intramolecular palladium-catalyzed ortho C-H activation/C-C cyclization and their antibacterial activityElectronic supplementary information (ESI) available: Experimental procedures and compound characterization data, and 1H and 13C NMR spectra of new compounds (PDF). See DOI: 10.1039/c6ob02707e