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6039
Titelbild: Erste strukturelle Charakterisierung eines binären P‐N‐Moleküls: die hochenergetische Verbindung P3N21 (Angew. Chem. 36/2006)
Göbel, Michael
/ Karaghiosoff, Konstantin
/ Klapötke, Thomas M.et al.
| 2006
Simplified Analysis of Mixtures of Small Molecules by Chromatographic NMR Spectroscopy. This study was supported in part by a grant from the French Conseil Régional Provence-Alpes-Côte-d'Azur and the Pharmaceutical Laboratory DistriB3 (Marseille, France). We thank VWR International France for providing all chromatographic stationary phases used herein.
Synthesis and Structure of the "Dialuminyne" Na2[Ar'AlAlAr'] and Na2[(Ar''Al)3]: AlAl Bonding in Al2Na2 and Al3Na2 Clusters. We thank the National Science Foundation for financial support. We also thank Dr. J. C. Fettinger and Dr. R. Fischer for assistance with crystallographic and NMR studies. Ar'=C6H3-2,6-(C6H3-2,6-iPr2)2; Ar''=C6H3-2,6-(C6H2-2,4,6-Me3)2.
Photochemical Upconversion: Anthracene Dimerization Sensitized to Visible Light by a RuII Chromophore. F.N.C. gratefully acknowledges financial support from the US Air Force Office of Scientific Research (FA9550-05-1-0276), the US National Science Foundation (CAREER Award CHE-0134782), the American Chemical Society (44138-AC3), and the BGSU Technologies Innovations Enhancement Program.
Proton-Fueled, Reversible Assembly of Gold Nanoparticles by Controlled Triplex Formation. This work was supported by a Korea Research Foundation grant funded by the Korea Government (MOEHRD, Basic Research Promotion Fund; KRF-2005-070-C00078). We thank Professor Younghoon Lee of the Department of Chemistry at KAIST for help with the experiments. Y.-G.K. is grateful for financial support from the Basic Research Program of the Korea Science and Engineering Foundation (grant no. R01-2006-000-11187-0)
Manganese Oxide Nanoparticles Electrodeposited on Platinum Are Superior to Platinum for Oxygen Reduction. Financial support by New Energy and Industrial Technology Development Organization (NEDO), Japan is greatly acknowledged.
Luminescence Studies of the Intracellular Distribution of a Dinuclear Gold(I) N-Heterocyclic Carbene Complex. Financial support for this work was provided by an Australian Research Council Discovery grant. Use of the ChemMat-CARS Sector 15 at the Advanced Photon Source was supported by the Australian Synchrotron Research Program, which is funded by the Commonwealth of Australia under the Major National Research Facilities Program. Chem-MatCARS Sector 15 is also supported by the National Science Foundation-Department of Energy under Grant Nos. CHE9522232 and CHE0087817 and by the Illinois Board of Higher Education. The Advanced Photon Source is supported by the US Department of Energy, Basic Energy Sciences, Office of Science, under Contract No. W-31109-Eng-38. We thank Dr Ron Clarke for very helpful discussions on the luminescence studies.
Metal-Compound-Induced Vesicles as Efficient Directors for Rapid Synthesis of Hollow Alloy Spheres. This work was partly supported by the National Natural Science Foundation of China (Nos. 20571050 and 20271031), the China Postdoctoral Science Foundation, and the NSF of Guangdong Province (No. 05300875).
Metal-Organic Frameworks as Efficient Materials for Drug Delivery. The authors are grateful to E. Fraga (C.A.I. of XRF spectroscopy, Complutense University) for collecting the X-ray fluorescence (XRF) spectra. Ibuprofen was kindly supplied by Laboratorios Dr. Esteve S.A.
Direct Monitoring of the Asymmetric Induction of Solid-Phase Catalysis Using Circular Dichroism: Diamine-CuI-Catalyzed Asymmetric Henry Reaction. This work was supported by a Grant-in Aid for Scientific Research from the Ministry of Education, Science, Sports, Culture and Technology of the Japanese Government and the Industrial Technology Research Grant Program in 2006 from the New Energy and Industrial Technology Development Organization (NEDO) of Japan.
Highly Efficient Asymmetric Michael Addition of Aldehydes to Nitroalkenes Catalyzed by a Simple trans-4-Hydroxyprolylamide. This work was financially supported by The University of the Basque Country (UPV-EHU) and the Ministerio de Educacion y Ciencia (MEC, Spain). A predoctoral grant to S.V. from MEC is also acknowledged. We also thank M. Alcalá and A. Lizarraga for their help with some experimental work and the SGI-IZO-SGIker UPV-EHU for allocation of computational resources.
Activation of Aryl Germanium(II) Chlorides by [Mo(PMe3)6] and [W([eta]2-CH2PMe2)H(PMe3)4]: A New Route to Metal-Germanium Triple Bonds. We are grateful to the Humboldt-Universität zu Berlin and the Deutsche Forschungsgemeinschaft (project FI 445-6-1) for the generous financial support of this work, Dr. B. Ziemer and P. Neubauer for technical assistance with the X-ray diffraction studies, Dr. U. Hartmann and U. Kätel for the elemental analyses, and Dr. C. Mügge, W.-D. Bloedorn, A. Thiesies, C. Schmidt, and K. Prochnicki for NMR experiments. N.W. thanks the Fonds der Chemischen Industrie for a fellowship.
Gold(I)-Catalyzed Cyclizations of Silyl Enol Ethers: Application to the Synthesis of (+)-Lycopladine A. We gratefully acknowledge the University of California, Berkeley, NIHGMS (R01 GM073932-01), Merck Research Laboratories, Bristol-Myers Squibb, Amgen Inc., DuPont, GlaxoSmithKline, Eli Lilly & Co., Pfizer, AstraZeneca, and Roche for financial support. J.J.K.-S. thanks Eli Lilly & Co. for a graduate fellowship. We thank Lauren A. Young for the preparation of tributylallenylstannane.
b-Disubstituted Allylic Chlorides: Substrates for the Cu-Catalyzed Asymmetric SN2' Reaction. We thank the Swiss National Research Foundation (no. 200020-105368) and COST action D24-003-01 (OFES contract no. C02.0027) for financial support, and BASF for the generous gift of chiral amines.
Self-Regenerating Rh- and Pt-Based Perovskite Catalysts for Automotive-Emissions Control. We thank Prof. Emeritus Dr. M. Misono (Univ. of Tokyo) and Prof. Dr. T. Kobayashi (AIST) for their advice on catalyst research, and Dr. T. Uruga, Mr. K. Kato, and Ms. Y. Okajima (SPring-8) for their help with the XAFS experiments. We also thank Mr. A. Hirai, Mr. N. Sato, Mr. H. Suzuki, and Mr. S. Matsueda (Cataler), Mr. S. Mitachi and Mr. S. Araki (Hokko Chem.), and Dr. N. Kawase (NTC), Mr. K. Mitsumori, Mr. I Takahashi, and Mr. K. Naito (Daihatsu) for their cooperation in catalyst research and development. This work was supported by the Japan Ministry of Education, Culture, Sports, Science and Technology; KAKENHI (15350090).
Pd(OAc)2-Catalyzed Coupling-Cyclization of 2,3-Allenoic Acids and Methyl Propiolate: Observation of Double 1,7-Hydrogen Shifts. Financial support from the National Natural Science Foundation of China (20121202 and 20332060) and Shanghai Municipal Committee of Science and Technology is greatly appreciated. We thank Mr. Xuefeng Jiang for checking the results of entries 3 and 5 in Table 1 and Scheme 4.
Storing and Releasing Hydrogen with a Redox Switch. We thank the EPSRC (grant GR-T10169), the Royal Society, and the Rhodes Trust for support, Dr Damien Murphy (Cardiff University) for providing the EPR spectra, and the Oxford Supercomputing Centre for computational facilities.
Metallic Magnesium Nano-Mesoscale Structures: Their Shape-Controlled Preparation and Mg-Air Battery Applications. This work was supported by the NSFC (20325102 and 90406001) and the 973 Program (2005CB623607). W.L. and C.L. contributed equally to this work. We are also very grateful to the reviewers for their valuable suggestions.
Solid-State Phase Transition of an Inclusion Complex of 5-Methyl-2-pyridone with 1,3,5-Benzenetricarboxylic Acid. S.T. and F.T. are grateful for the financial support from MEXT.HAITEKU (2001-2005). H.U. is grateful to Professor K. D. M. Harris (Cardiff University, Wales) for supplying the program EAGER for structure solution from powder diffraction data, and to the financial support by Grant-in-Aid for Scientific Research (KAKENHI) in Priority Area "Molecular Nano Dynamics" from MEXT.
Anomeric Acetates of N-Acetylneuraminic Acid are Useful C-Sialyl Donors in Samarium-Mediated Reformatsky Coupling Reactions. We thank the Ministère de la Recherche for PhD grants to A.M. and Z.A.
N-Heterocyclic Carbene Catalyzed CC Bond Cleavage in Redox Esterifications of Chiral Formylcyclopropanes. This study was supported by the National Science Foundation (CHE-0449587) and the California Cancer Research Coordinating Committee. J.W.B. is grateful to Amgen and Richard and Leslie Anderson for additional support. We are grateful to Sean Riznikove, John Unger, and Bruce Lipshutz (UCSB) for assistance with the chiral GC analyses.
Enantioselective Catalytic Intramolecular Cyclopropanation using Modified Cinchona Alkaloid Organocatalysts. We gratefully acknowledge Pfizer Ltd (Sandwich) for a PhD studentship (C.C.C.J.), Syngenta for a Case Award (N.B.), Novartis for a Research Fellowship (S.V.L.), the Royal Society for University Research Fellowship (M.J.G.), and the EPSRC Mass Spectrometry service at the University of Swansea.
Gold(I)-Catalyzed Intermolecular Cyclopropanation of Enynes with Alkenes: Trapping of Two Different Gold Carbenes. We are grateful to the MEC (project CTQ2004-02869, Torres Quevedo (contract to S.L. and predoctoral fellowships to E.H.-G., P.P.-G., and C.N.-O.), the AGAUR (2005 SGR 00993), and the ICIQ Foundation for financial support.
Eigenschaftsorientiertes rationales Design von Einzelmolekülmagneten: ein aus drei molekularen Bausteinen aufgebauter Mn6Cr‐Komplex mit C3‐Symmetrie und einem Spingrundzustand von St=21/2
Eigenschaftsorientiertes rationales Design von Einzelmolekülmagneten: ein aus drei molekularen Bausteinen aufgebauter Mn6Cr-Komplex mit C3-Symmetrie und einem Spingrundzustand von St=21-2. Diese Arbeit wurde vom Fonds der Chemischen Industrie, dem BMBF, der Dr. Otto Röhm Gedächtnisstiftung und der DFG (SFB424 und SFB583) unterstützt. Wir danken Dr. E. Bill (MPI für Bioanorganische Chemie) für magnetische Messungen und anregende Diskussionen.
Eigenschaftsorientiertes rationales Design von Einzelmolekulmagneten: ein aus drei molekularen Bausteinen aufgebauter Mn6Cr-Komplex mit C3-Symmetrie und einem Spingrundzustand von St=21/2
Glaser, T.
/ Heidemeier, M.
/ Weyhermuller, T.et al.
| 2006
Erste strukturelle Charakterisierung eines binären P-N-Moleküls: die hochenergetische Verbindung P3N21. Wir danken Dr. G. Fischer für die Durchführung der Massenspektrometrie-Experimente und T. Kerscher für die Unterstützung bei den Rechnungen. M. Göbel dankt der bischöflichen Studienförderung Cusanuswerk für ein Promotionsstipendium. Der Ludwig-Maximilians-Universität und dem Fonds der chemischen Industrie sei für die finanzielle Unterstützung gedankt. Wir danken der Bundesrepublik Deutschland und dem Freistaat Bayern für die Beschaffung eines Einkristall-Diffraktometers im Rahmen des HBFG-Programms.
Effiziente Synthese funktionalisierter zinkorganischer Verbindungen durch direkte Insertion von Zink in organische Bromide und Iodide. Wir danken dem Fonds der Chemischen Industrie und den Merck Research Laboratories (MSD) sowie der DFG für finanzielle Unterstützung. Ebenso danken wir der Chemetall GmbH (Frankfurt) und der BASF AG (Ludwigshafen) für großzügige Chemikalienspenden.
Mechanistische Untersuchungen des Kettenwachstums von Polyethylen in Gegenwart von Wasser. Diese Arbeit wurde von der DFG (Me1388-3-2) unterstützt. Wir danken U. Haunz für die technische Unterstützung und H. Möller für Diskussionen zur NMR-Spektroskopie.
18F-Markierung von Peptiden mithilfe eines Organosilicium-Fluoridacceptors. Die Autoren danken der International Isotope Society Central European Division für finanzielle Unterstützung. Die Autoren danken weiterhin Philips für Unterstützung und Herrn Prof. Dr. H. J. Wester (TU München) für ein Syntheseprotokoll zur Oximbildung. C.M.N. und G.B. danken dem Zentrum für Angewandte Chemische Genomik, einer Forschungsinitiative der Europäischen Union und des Ministeriums für Innovation und Forschung des Landes Nordrhein-Westfalen, für finanzielle Unterstützung.
Li26-Cluster in der Verbindung Li13Na29Ba19. Wir danken Dr. C. Hoch für die Aufnahme der Einkristalldaten und Dr. J. Köhler für hilfreiche Diskussionen.
Die regioselektive eisenkatalysierte allylische Aminierung. Herrn Prof. Dr. N. Krause sowie dem Fonds der Chemischen Industrie, der Deutschen Forschungsgemeinschaft, der Dr.-Otto-Röhm-Gedächtnisstiftung und dem Fonds zur Förderung des wissenschaftlichen Nachwuchses im Fachbereich Chemie der Universität Dortmund sei für die großzügige Unterstützung unserer Arbeiten gedankt.