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6085
Titelbild: Oxygen Atom Transfer in the Photocatalytic Oxidation of Alcohols by TiO2: Oxygen Isotope Studies (Angew. Chem. 33/2009)
Dendritische DNA-Bausteine für Amplifizierungs-Nachweisassays und Biomaterialien Die Autoren danken der Deutschen Forschungsgemeinschaft für finanzielle Unterstützung der Projekte FE 943-1-1, SA 1952-1-1 und NI 399-10-1. Wir danken Kersten S. Rabe für viele hilfreiche Diskussionen.
Chiralitätstransfer als Zugang zu oxygenierten gewinkelten aromatischen Polyketiden Wir danken den National Institutes of Health für die Unterstützung.
Totalsynthese des Antibiotikums Kendomycin durch Photo-Fries-Umlagerung und Ringschlussmetathese Wir danken Dr. Lothar Brecker und Susanne Felsinger für die Aufnahme und Interpretation von NMR-Spektren und Prof. A. Zeeck für eine authentische Probe von 1.
Oxidation von Catecholborenolaten mit TEMPO Wir danken dem Fonds der Chemischen Industrie (Stipendium für T.V.), Novartis Pharma AG (Young Investigator Award für A.S.), der DFG (A.S.) und dem Schweizerischen Nationalfonds (P.R.) für finanzielle Unterstützung. Ciba Spezialitätenchemie und BASF SE danken wir für Chemikalienspenden.
Eisen-katalysierte Carbonylierungen: selektive und effiziente Synthese von Succinimiden Diese Arbeit wurde durch das Land Mecklenburg-Vorpommern, das BMBF (Bundesministerium für Bildung und Forschung) und die DFG (Graduiertenkolleg 1213 und Leibniz-Preis) unterstützt. Wir danken Dr. W. Baumann, Dr. C. Fischer, S. Buchholz, S. Schareina und K. Mevius für ihre technische und analytische Unterstützung.
Rutheniumkatalysierte regioselektive direkte Alkylierungen von Arenen mit nichtaktivierten Alkylhalogeniden unter C-H-Bindungsspaltung Wir danken der DFG und der Alexander von Humboldt-Stiftung (Stipendium für R.V.) für großzügige Unterstützung.
Nucleotide-Catalyzed Conversion of Racemic Zeolite-Type Zincophosphate into Enantioenriched Crystals We acknowledge the support of this work by the NIH (X.B., 2 S06 GM063119-05). X.B is a Henry Dreyfus Teacher Scholar.
Rhodium-Catalyzed Enantioselective and Diastereoselective Hydrogenation of β-Ketoenamides: Efficient Access to anti 1,3-Amino Alcohols This research was supported by the National Institutes of Health (GM58832), China Scholarship Council, and Northwest Agriculture & Forestry University. Mass spectrometry was carried out by the Washington University Mass Spectrometry Resource, an NIH Research Resource (Grant P41RR0954).
A Ferromagnetic [Cu3(OH)2]4+ Cluster Formed inside a Tritopic Nonaazapyridinophane: Crystal Structure and Solution Studies MCINN is gratefully acknowledged for financial support, project nos. CTQ-BU-015672-CO-O1-02, CTQ-BQU-2005-08123-CO2-02, MAT2006-01997, CTQ-PPQ-2007-61126, Factoría de Cristalización Consolider Ingenio 2010 and the Catalan Government (2005SGR-00036)as well as FEDER fundings. J.C. thanks the University of Valencia for a Mobility Program grant to cover his stay as Invited Professor in Valencia. The authors thankfully acknowledge the computer resources, technical expertise, and assistance provided by the Barcelona Supercomputing Center (Centro Nacional de Supercomputación) and SCTs-Universidad de Oviedo)
Titanosilsesquioxanes Embedded in Synthetic Clay as a Hybrid Material for Polymer Science We acknolowedge financial support from MIUR (PRIN Project "Progettazione e sintesi di Silsesquiossani Poliedrici Multifunzionali per Compositi Polimerici Innovativi Termicamente Stabili") and from Regione Piemonte (Progetto NANOMAT, Docup 2000-2006, Linea 2.4a). We thank Prof. Giovanni Talarico (Dipartimento di Chimica "Paolo Corradini", Università di Napoli "Federico II") for computational analysis and Aman Ullah (Dipartimento di Chimica e Chimica Industriale, Università di Genova) for preparation of the polystyrene-based nanocomposite.
Highly Regio- and Enantioselective Copper-Catalyzed Hydroboration of Styrenes This research was supported by a Korea Science and Engineering Foundation (KOSEF) grant funded by the Korean government (MEST; No. R01-2008-000-20332-0).
Regulating Copper-Binding Affinity with Photoisomerizable Azobenzene Ligand by Construction of a Self-Assembled Monolayer We acknowledge Prof. Hideki Masuda and Dr. Tomohiko Inomata (Nagoya Institute of Technology) for the preparation of Au substrates, and Dr. Akiharu Satake (Nara Institute of Science and Technology) for help with the NMR measurements. This work was partially supported by Grants-in-Aid for Scientific Research (No. 21350095) to S.H. and on Priority Areas (No. 20051016) from MEXT and TRPCO Research Foundation. I.T. is financially supported as an Inoue Fellow from the Inoue Foundation for Science.
Size-Controlled Synthesis of Conducting-Polymer Microspheres by Pulsed Sonoelectrochemical Polymerization This work was partially supported by the Global COE program (Tokyo Institute of Technology) and a Grant-in-Aid for Scientific Research (20350046 and 21656205) from the Japanese Ministry of Education, Science, Culture, and Sports.
Axial Chirality Control of Gold(biphep) Complexes by Chiral Anions: Application to Asymmetric Catalysis This work was supported by a Grant-in-Aid for Scientific Research on Priority Area "Advanced Molecular Transformations of Carbon Resources" from the Ministry of Education, Culture, Sports, Science and Technology (Japan). We thank Dr. K. Hasegawa of Rigaku Co. for the X-ray analyses.
Oxygen Atom Transfer in the Photocatalytic Oxidation of Alcohols by TiO2: Oxygen Isotope Studies This work was supported by 973 project (No. 2007CB613306), NSFC (Nos. 20537010, 20772129 and 20877076) and CAS.
SiC: A Photocathode for Water Splitting and Hydrogen Storage We thank Bas Opperdoes for MBE assistance and Hans Ligthart and Rinus Mackaay for technical support. This work was financially supported by the Dutch Technology Foundation (STW, UPC-6317).
Highly Stereoselective One-Pot Synthesis of Bicyclic Isoxazolidines with Five Stereogenic Centers by an Organocatalytic Process Research support from the Ministry of Education in Singapore (ARC12-07, no. T206B3225) and Nanyang Technological University (URC, RG53-07) is gratefully acknowledged. We thank Dr. Yongxin Li for the X-ray crystallographic analysis.
Selectivity Control in Lewis Acid Catalyzed Regiodivergent Tandem Cationic Cyclization-Ring Expansion Terminated by Pinacol Rearrangement We are grateful to the NSFC (20702015) for financial support. This work was also sponsored by the 973 program (2009CB825300), the Shanghai Shuguang Program (07SG27), the Shanghai Pujiang Program (07pj14039), and the Shanghai Leading Academic Discipline Project (B409).
Palladium(II)-Catalyzed ortho Alkylation of Benzoic Acids with Alkyl Halides We thank The Scripps Research Institute, the U.S. National Institutes of Health (NIGMS, 1 R01 GM084019-01A1), Amgen, and Lilly for financial support, and the A. P. Sloan Foundation for a fellowship (J.-Q.Y.).
Heck Reactions with Palladium Nanoparticles in Ionic Liquids: Coupling of Aryl Chlorides with Deactivated Olefins This research was in part financially supported by the University of Bari.
Total Synthesis of Celogentin C We thank Brigham Young University and the National Institutes of Health (GM70483) for support of this work. We also thank Prof. Hiroshi Morita of Hoshi University for providing an analytical sample of celogentin C and Joshua W. Robinson for assistance in preparing compound 2.
Benzo- and Naphthoborepins: Blue-Emitting Boron Analogues of Higher Acenes Funding for this work was provided by NSERC of Canada and the Xerox Research Foundation.
Selective Synthesis of [12]Cycloparaphenylene This work was supported by the PRESTO program of the Japan Science and Technology Agency (JST), and a Grant-in-Aid for Scientific Research from MEXT and JSPS. J.B. is a recipient of a JSPS Postdoctoral Fellowship. We thank Dr. Kin-ichi Oyama (Nagoya University) for assistance in MALDI-TOF MS analysis, Prof. Yasuhiro Ohki and Prof. Kazuyuki Tatsumi (Nagoya University) for assistance in X-ray crystal structure analysis, and Prof. Atsushi Wakamiya and Prof. Shigehiro Yamaguchi (Nagoya University) for useful discussion and technical assistance. Last but not least, we thank the late Kazuhiko Seki (Nagoya University) for his encouragement.
Indium-Based Perovskites: A New Class of Near-Room-Temperature Multiferroics This work was supported by World Premier International Research Center (WPI) Initiative on Materials Nanoarchitectonics (MEXT (Japan)) and by the NIMS Individual-Type Competitive Research Grant. We thank Drs. H. Yoshikawa and K. Kobayashi of NIMS for their suggestions and encouragement and Drs. Y. Katsuya and J. Kim and Ms. J. Uchida of SPring-8 for their support for SXRD. Some SXRD experiments were performed under the proposal 2009A1136.
Chemoselectivity in Catalytic C&bond;C and C&bond;H Bond Activation: Controlling Intermolecular Carboacylation and Hydroarylation of Alkenes We acknowledge the donors of the ACS Petroleum Research Fund for partial support (47565-G1). We thank Dr. Letitia Yao (NMR spectroscopy), Matthew Meyer and Jacob Schmidt (mass spectrometry), and UMN (start-up funds).
Network Topology of a Hybrid Organic Zinc Phosphate with Bimodal Porosity and Hydrogen Adsorption This research was supported by the National Science Council NSC-97-2113-M007-013-MY3, NSC-97-2113-M-033-003-MY2, Chung Yuan Christian University (CYCU-97-CR-CH), and the National Synchrotron Radiation Research Center of Taiwan (Contract No. 2007-3-089-4).
Segmental Isotopic Labeling of a Central Domain in a Multidomain Protein by Protein Trans-Splicing Using Only One Robust DnaE Intein We thank the Protein Chemistry Research Group at the Institute of Biotechnology and Dr. Ute Bahr for mass spectrometry analysis. This work was supported by the grants from the Academy of Finland (118385), Sigrid Jusélius Foundation, the Center for Biomolecular Magnetic Resonance (BMRZ), and the Cluster of Excellence Frankfurt (CEF).
A Color-Tunable Europium Complex Emitting Three Primary Colors and White Light This work is supported by the National Natural Science foundation of China (20571041 and 20501016) and the Start-up Fund of The Dalian University of Technology.
Direct Observation of Contact Ion-Pair Formation in Aqueous Solution We thank Dr. Soenke Seifert (XSD-APS-ANL) for assistance with the SAXS measurements and Dr. Nate Ockwig for assistance in data collection. This work is supported by the U. S. Department of Energy, Office of Basic Energy Science, Division of Chemical Sciences, Biosciences and Geosciences, under contract no. DE-AC02-06CH11357, for the part performed at Argonne National Laboratory. We are grateful to Mona Aragon (SNL) for assistance with graphics. Sandia authors thank the LDRD program for financial support. Sandia is a multiprogram laboratory operated by Sandia Corporation, a Lockheed-Martin Company, for the United States Department of Energy under Contract No. DE-AC04-94AL85000.
Rotational Spectral Signatures of Four Tautomers of Guanine This research was supported by the Ministerio de Educación y Ciencia (MEC, grant CTQ2006-05981-BQU) and the Junta de Castilla y León (grant VA070A08).
Self-Assembled ABC Triblock Copolymer Double and Triple Helices G.L. thanks the NSERC of Canada for sponsoring this research. H.J. thanks the Ministry of Education, Science, Sports and Culture for support through Grants-in-aid 19031016, 21015017, and 21241030.
Electrophilic Activation of Benzaldehydes through ortho Palladation: One‐Pot Synthesis of 3‐Methylene‐indan‐1‐ols through a Domino Allylstannylation/Heck Reaction under Neutral Conditions
Electrophilic Activation of Benzaldehydes through ortho Palladation: One-Pot Synthesis of 3-Methylene-indan-1-ols through a Domino Allylstannylation-Heck Reaction under Neutral Conditions This work was supported by the Universität zu Köln.
Evolution of Propargyl Ethers into Allylgold Cations in the Cyclization of Enynes This work was supported by the MEC (projects CTQ2004-02869, Consolider Ingenio 2010 Grant CSD2006-0003, predoctoral fellowships to E.J.-N, M.R., C.R.S., Juan de la Cierva Contract to T.L.), and the ICIQ Foundation. We also thank Dr. J. Benet-Buchholz and E. Escudero-Adán (X-ray diffraction unit, ICIQ) for the structures of 2 f, 7 f, and 22 a.
Copper(I) Cuboctahedral Coordination Cages: Host-Guest Dependent Redox Activity This work was supported by the NSFC for Distinguished Young Scholars (20525310) and Innovative Groups (20821001), 973 Program of China (2007CB815302), the NSFC Projects (20673147, 20773167, 20731005) and RFDP of Higher Education.
Size‐Selective Sorption of Small Organic Molecules in One‐Dimensional Channels of an Ionic Crystalline Organic–Inorganic Hybrid Compound Stabilized by π–π Interactions
Size-Selective Sorption of Small Organic Molecules in One-Dimensional Channels of an Ionic Crystalline Organic-Inorganic Hybrid Compound Stabilized by p-p Interactions
Size-Selective Sorption of Small Organic Molecules in One-Dimensional Channels of an Ionic Crystalline Organic-Inorganic Hybrid Compound Stabilized by π-π Interactions This work was supported by the Core Research for Evolutional Science and Technology (CREST) program of Japan Science and Technology Agency (JST), and Grants-in-Aid for Scientific Research and The University of Tokyo Global COE Program (Chemistry through Cooperation of Science and Engineering) from the Ministry of Education, Culture, Sports, Science, and Technology (MEXT) of Japan.
Trimeric Cyclic Assemblies of Calix[4]arene-Tethered Bismerocyanines This work was supported by the Deutsche Forschungsgemeinschaft (grant project: Wu 317-1-5 and postdoctoral fellowship for S.U. within the Research Training School 1221). We thank Dr. M. Büchner for MS measurements.