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3635
Titelbild: Hoch enantioselektive Aza‐Baylis‐Hillman‐Reaktion in einem chiralen Reaktionsmedium (Angew. Chem. 22/2006)
Insertion von Arinen in [sigma]-Bindungen. Die Autoren danken dem Spanischen Ministerium für Erziehung und Wissenschaft (MEC, CTQ2004-05752), FEDER und der Xunta de Galicia (DXID, 05PXIC20904PN) für die finanzielle Unterstützung. D. Peña dankt dem MEC für einen Ramon y Cajal-Forschungsvertrag.
Stickstoffreiche energetische Salze und ionische Flüssigkeiten. J.M.S. dankt AFOSR (F49620-03-1-0209), NSF (CHE0315275) und ONR (N00014-02-1-0600) für die finanzielle Unterstützung der Arbeiten an der University of Idaho.
A Nickel-Alkyl Bond in an Inactivated State of the Enzyme Catalyzing Methane Formation. We thank the Swiss National Science Foundation (SNF) and the Fonds der Chemischen Industrie for financial support. D.H. gratefully acknowledges a research scholarship (HI 1094-1-1) from the Deutsche Forschungsgemeinschaft (DFG). We are grateful to Brian M. Hoffman (Northwestern Univ.) for helpful discussions.
High-Throughput Carbohydrate Microarray Analysis of 24 Lectins. We thank Jack Simpson (Protein Chemistry Laboratory, SAIC-NCI-Frederick) for MALDI-MS analysis of BSA conjugates. This research was supported by the Intramural Research Program of the NIH, NCI.
Epitaxial Growth of Peptide Nanofilaments on Inorganic Surfaces: Effects of Interfacial Hydrophobicity-Hydrophilicity. We thank Dr. Bin Li, Xing-Fei Zhou, Yun-Chang Guo, and Hai Li for valuable discussions and Miss Stefanie Maerz for the helpful revisions. This work was supported by grants from the Shanghai Institute of Applied Physics, the National Natural Science Foundation of China (No. 10335070, 10404032, and 30400064), and the Science and Technology Commission of Shanghai Municipality (No. 04qmx1466 and 0552nm033).
Ultrastable Gold Nanocatalyst Supported by Nanosized Non-Oxide Substrate. This work was conducted at the Oak Ridge National Laboratory and supported by the Division of Chemical Sciences, Office of Basic Energy Sciences, US Department of Energy, under contract no. DE-AC05-00OR22725 with UT-Battelle, LLC. We thank the SHARE Facility at ORNL for the transmission electron microscopy. This research was supported in part by an appointment for W.F.Y. to the ORNL Postdoctoral Research Associates Program, administered jointly by the Oak Ridge Institute for Science and Education and ORNL.
Enhanced Signals and Fast Nucleic Acid Hybridization By Microfluidic Chaotic Mixing. This research was supported by the NIH Director's Pioneer Award (7DP1 0D000251-02) and NIH 1R01 HG002644-01A1. We thank Yanxia Hao and Dr. Christopher S. Baker of the Genomics Core Laboratory, Gladstone Institutes for providing mouse-printed oligoarrays (17 K) and Frederick Balagadde of Caltech for technical assistance.
Watson-Crick Base-Pairing Properties of Nucleic Acid Analogues with Stereocontrolled [alpha] and b Torsion Angles ([alpha],b-D-CNAs). We thank the Centre Informatique National de l'Enseignement Supérieur (CINES) and the Centre Interuniversitaire de Calcul de Toulouse (CALMIP) for the generous allocation of computer time and Dr. M. Erard for assistance with the CD experiments. D-CNAs=constrained nucleic acids with dioxaphosphorinane ring.
A New Reaction Pathway in Organophosphorus Chemistry: Competing SN2 and AE' Pathways for Nucleophilic Attack at a Phosphorus-Carbon Cage Compound. We acknowledge the EPSRC (R.J.K., D.A.P., C.E.W.), the Universities of Bristol (M.G., C.A.R., C.F.) and York (C.E.W., J.M.L.), and The Royal Society (University Research Fellowship for C.A.R.) for financial assistance. We thank Dr. Craig Butts (Bristol) for helpful comments in preparing this manuscript.
Surface Plasmon Resonances of Free-Standing Gold Nanowires Fabricated by Nanoskiving. This research was supported by the NIH (GM065364), by DARPA (sub-award to G.M.W. from the Center for Optofluidic Integration at the California Institute of Technology), and by a MURI AFOSR sub-award to F.C. MRSEC and NSEC shared facilities supported by the NSF under awards DMR-0213805 (MRSEC) and PHY-0117795 (NSEC) were utilized. We thank Ertugrul Cubukcu, Dr. Marko Loncar, Dr. Brian Mayers, and Prof. Kenneth Crozier for helpful discussions.
Short Synthesis of Skeletally and Stereochemically Diverse Small Molecules by Coupling Petasis Condensation Reactions to Cyclization Reactions. The NIGMS-sponsored Center of Excellence in Chemical Methodology and Library Design (Broad Institute CMLD) enabled this research. We thank Nilesh Kumar and Drs. Paul Clemons, Ryan Looper, Xiang Wang, and Damian Young for helpful discussions. G.M. is a visiting PhD student from the Dipartimento Farmacochimico, University of Bari (Italy). S.L.S. is an Investigator with the Howard Hughes Medical Institute.
Controlled Self-Assembly Behavior of an Amphiphilic Bisporphyrin-Bipyridinium-Palladium Complex: From Multibilayer Vesicles to Hollow Capsules. This work was supported by the National Natural Science Foundation of China (20531060, 10474101, 20418001, 20571078, and 20421101), and the Major State Basic Research Development Program (2005CB623602). This project is partly supported by National Center for Nanoscience and Technology, China.
Cyclophanes within Cyclophanes: The Synthesis of a Pyromellitic Diimide‐Based Macrocycle as a Structural Unit in a Molecular Tube and Its Inclusion Phenomena
Cyclophanes within Cyclophanes: The Synthesis of a Pyromellitic Diimide-Based Macrocycle as a Structural Unit in a Molecular Tube and Its Inclusion Phenomena. Molecular Tubes and Capsules, Part 1. We gratefully acknowledge the financial support by a Theme Project of Molecular Architecture of Organic Compounds for Functional Design (Prof. Tahsin J. Chow) from the Institute of Chemistry, Academia Sinica, Taiwan R.O.C. We are also grateful for partial financial support by the Joint Project of Chemical Synthesis Core Research Institutions, Research and Education for Inter-University Research Project, MEXT, Japan.
AuI-Catalyzed Tandem [3,3] Rearrangement-Intramolecular Hydroarylation: Mild and Efficient Formation of Substituted Indenes. The National Science Foundation is gratefully acknowledged for financial support of this work. S.D.G. thanks the Education, Research, and Universities Department of the Basque Government (Spain) for a postdoctoral fellowship. We also thank the Department of Chemistry of the University of Ottawa, and more specifically Prof. Deryn Fogg, for hosting our group while the University of New Orleans was recovering from Hurricane Katrina. Degussa AG, Umicore AG, and Strem are also gratefully acknowledged.
Total Synthesis of (+)-Machaeriol D with a Key Regio- and Stereoselective SN2' Reaction. We are grateful for the financial support of the NSFC (No. 20572036, QT program), the Special Doctorial Program Funds of the Ministry of Education of China (20040730008), GanSu Science Foundation (No. 3ZS051A25-004), and the Key Grant Project of the Ministry of Education of China (No.105169).
A Nanowire-Nanoparticle Cross-Linking Approach to Highly Porous Electrically Conducting Solids. This work was supported by a grant (CTS 04-27418) from the National Science Foundation. We thank Prof. Susan Kauzlarich for providing a furnace for the synthesis of starting materials.
A General Synthesis of C6-Azolyl Purine Nucleosides. This work was supported by a National Institutes of Health grant (no.: S06 GM008168-24S1), partially by a National Science Foundation (NSF) grant (no.: CHE-0314326), and by a PSC-CUNY36 award. Acquisition of a 500 MHz NMR spectrometer and a mass spectrometer was funded by NSF grants (nos.: CHE-0210295 and CHE-0520963, respectively). Dr. P. Pradhan is thanked for his assistance.
Hydrogen-Isotope Scrambling on Doped Sodium Alanate. This work was partially supported by General Motors Fuel Cell Activities, in addition to the basic funding by the Max-Planck-Gesellschaft.
Protected 32P‐Labels in Deoxyribonucleotides: Investigation of Sequence Selectivity of DNA Photocleavage by Enediyne–, Fulvene–, and Acetylene–Lysine Conjugates
Breiner, Boris
/ Schlatterer, Jörg C.
/ Kovalenko, Serguei V.et al.
| 2006
Protected 32P-Labels in Deoxyribonucleotides: Investigation of Sequence Selectivity of DNA Photocleavage by Enediyne-, Fulvene-, and Acetylene-Lysine Conjugates. I.A. is grateful to the National Science Foundation (grant no.: CHE-0316598) for partial support of this research and to the 3M Company for an Untenured Faculty Award. N.L.G. thanks the National Science Foundation (grant no.: MCB 0316494) and the National Institutes of Health (grant no.: RO1 GM54008) for their support. We are also grateful for technical support from Dr. L. Keller (Florida State University Biology Department).
Subpyriporphyrin-A [14]Triphyrin(1.1.1) Homologue with an Embedded Pyridine Moiety. Financial support from the Ministry of Scientific Research and Information Technology (Grant 3T09A16228) is gratefully acknowledged. Quantum mechanical calculations were preformed at the Supercomputer Centers in Wroclaw and Poznan.
Designed CO2-Philes Stabilize Water-in-Carbon Dioxide Microemulsions. S.G., A.G., and S.R. thank the University of Bristol DTA, CNPq Brazil, and EPSRC (EP-C523105-1) for studentships and a post-doctoral fellowship, respectively. CCLRC are thanked for beam time and consumables-travel grants. Alan Pitt (Kodak (UK)) is thanked for stimulating discussions. The University of Pittsburgh would like to express its appreciation to the US DOENETL for supporting this research through contract DE-FG26-04NT-15533.
Chiral 4-Phenyl-2-trifluoromethyloxazolidine: A High-Performance Chiral Auxiliary for the Alkylation of Amides. We thank the French ministry of research for awarding a research fellowship to A.T. and the Central Glass Company for the generous gift of trifluoroacetaldehyde hemiacetal.
Eine hoch enantioselektive Bronsted-Saure-katalysierte Kaskadenreaktion: organokatalytische Transferhydrierung von Chinolinen und deren Anwendung in der Synthese von Alkaloiden
Rueping, M.
/ Antonchick, A. P.
/ Theissmann, T.et al.
| 2006
Eine hoch enantioselektive Brønsted-Säure-katalysierte Kaskadenreaktion: organokatalytische Transferhydrierung von Chinolinen und deren Anwendung in der Synthese von Alkaloiden. Die Autoren danken der Degussa AG für die großzügige Unterstützung.
Eine hoch enantioselektive Brønsted‐Säure‐katalysierte Kaskadenreaktion: organokatalytische Transferhydrierung von Chinolinen und deren Anwendung in der Synthese von Alkaloiden
Rueping, Magnus
/ Antonchick, Andrey P.
/ Theissmann, Thomaset al.
| 2006
Kupfer-katalysierte Synthese von Ketonen mit [alpha]-stereogenem Zentrum. Wir danken dem Fonds der Chemischen Industrie, der Deutschen Forschungsgemeinschaft (KN347-6-2) und den Merck Research Laboratories für die finanzielle Unterstützung. Ebenso danken wir der Chemetall und der BASF für großzügige Chemikalienspenden.
Hoch enantioselektive Aza-Baylis-Hillman-Reaktion in einem chiralen Reaktionsmedium. Diese Arbeit wurde unterstützt von der Deutsche Forschungsgemeinschaft (SPP 1179, SFB 380). R.G. und P.B. danken dem Fonds der Chemischen Industrie und dem Graduiertenkolleg 440 "Methoden in der Asymmetrischen Synthese" für ein Promotionsstipendium. Wir danken Dr. K. Ditrich (BASF AG) für die großzügige Spende von (R)-Mandelsäure. Darüber hinaus möchten wir uns sehr bei H. Eschmann und T. Steins für die technische Unterstützung bedanken.
Größenabhängiger Oxidationsmechanismus trägerfixierter Pd-Nanopartikel. Diese Arbeit wurde von der Deutschen Forschungsgemeinschaft (SPP 1091) und dem Fonds der Chemischen Industrie gefördert.
Die Assoziation von Wasser in ionischen Flüssigkeiten: eine verlässliche Sonde zur Bestimmung der Polarität. Diese Arbeit wurde unterstützt vom Land Mecklenburg-Vorpommern (Hochschulwissenschaftsprogramm) und der DFG (FOR 436).
Die phosphanstabilisierten Gold‐Arsen‐Cluster [Au19(AsnPr)8(dppe)6]Cl3, [Au10(AsnPr)4(dppe)4]Cl2, [Au17(AsnPr)6(As2nPr2)(dppm)6]Cl3 und [Au10(AsPh)4(dppe)4]Cl2 – Synthese, Charakterisierung und DFT‐Rechnungen
Die phosphanstabilisierten Gold-Arsen-Cluster [Au19(AsnPr)8(dppe)6]Cl3, [Au10(AsnPr)4(dppe)4]Cl2, [Au17(AsnPr)6(As2nPr2)(dppm)6]Cl3 und [Au10(AsPh)4(dppe)4]Cl2 - Synthese, Charakterisierung und DFT-Rechnungen. Diese Arbeit wurde von der Deutschen Forschungsgemeinschaft (Centrum für Funktionelle Nanostrukturen), dem Deutsch-Israelischen Programm (DIP) und dem Fonds der Chemischen Industrie gefördert. dppe=1,2-Bis(diphenylphosphanyl)ethan, dppm=Bis(diphenylphosphanyl)methan.
Die höchsten Oxidationszustände der 5d-Elemente: der Fall Iridium(+VII). Wir danken M. Straka, R. Reviakine und M. Patzschke für hilfreiche Kommentare und technische Unterstützung.